Ignition finished(retried) [Error Code:9011]

Cause¶

Detector ignition sequence was re-attempted, because the ignition failed initially.

Solution¶

Check the following items.

• Check for gas leaks.

• Verify the gas flows.
  

  	Hydrogen	Air	Makeup Gas (BID : DCG) (ECD : ECD gas)	Note
  FID (Capillary column)	32.0 mL/min	200.0 mL/min	24.0 mL/min	--
  FID (Packed column)	32.0 mL/min	200.0 mL/min	Total flow rate of carrier gas and makeup gas : 20 to 50 mL/min	--
  FTD (N-mode)	1.0 to 2.0 mL/min	140.0 to 150.0 mL/min	10.0 to 30.0 mL/min	--
  FTD (P-mode)	3.0 to 6.0 mL/min	140.0 to 150.0 mL/min	10.0 to 30.0 mL/min	--
  FPD (P-mode)	62.5 mL/min	90.0 mL/min	--	--
  FPD (S-mode)	40.0 mL/min	60.0 mL/min	--	--
  FPD (Sn-mode)	75.0 mL/min	65.0 mL/min	--	--
  ECD	--	--	15.0 mL/min (Flow path A)*1 30.0 mL/min (Flow path B)*1	Nitrogen (N2) is used
  BID	--	--	Depends on the column flow rate. Less than10.0 mL/min : 50.0 mL/min 10.0 mL/min to15.0 mL/min : 70.0 mL/min More than 15.0 mL/min : 100.0 mL/min	Helium (He) is used
  SCD	80.0 mL/min	--	40.0 mL/min	Oxygen for he furnace : 10.0 mL/min Oxygen for the ozone generator : 25.0 mL/min

  
  *1 ECD-2010 Exceed column insertion length differs depending on the flow path. Refer to Method for distinguishing the different ECD-2010 Exceed flow paths to determine the flow path.

• Diagnose ignition pulse and ignition sequence by standard diagnosis.
  [Standard Diagnosis] Screen

If this massage appears frequently after checking above items, contact your Shimadzu sales/service representative.