Ignition finished(retried) [Error Code:9011]
Cause¶
Detector ignition sequence was re-attempted, because the ignition failed initially.
Solution¶
Check the following items.
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Check for gas leaks.
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Verify the gas flows.
HydrogenAirMakeup Gas
(BID : DCG)
(ECD : ECD gas)NoteFID
(Capillary column)32.0 mL/min200.0 mL/min24.0 mL/min--FID
(Packed column)32.0 mL/min200.0 mL/minTotal flow rate of carrier gas and makeup gas : 20 to 50 mL/min--FTD
(N-mode)1.0 to 2.0 mL/min140.0 to 150.0 mL/min10.0 to 30.0 mL/min--FTD
(P-mode)3.0 to 6.0 mL/min140.0 to 150.0 mL/min10.0 to 30.0 mL/min--FPD
(P-mode)62.5 mL/min90.0 mL/min----FPD
(S-mode)40.0 mL/min60.0 mL/min----FPD
(Sn-mode)75.0 mL/min65.0 mL/min----ECD----15.0 mL/min (Flow path A)*1
30.0 mL/min (Flow path B)*1Nitrogen (N2) is usedBID----Depends on the column flow rate.
Less than10.0 mL/min : 50.0 mL/min
10.0 mL/min to15.0 mL/min : 70.0 mL/min
More than 15.0 mL/min : 100.0 mL/minHelium (He) is usedSCD80.0 mL/min--40.0 mL/minOxygen for he furnace : 10.0 mL/min
Oxygen for the ozone generator : 25.0 mL/min
*1 ECD-2010 Exceed column insertion length differs depending on the flow path. Refer to Method for distinguishing the different ECD-2010 Exceed flow paths to determine the flow path. -
Diagnose ignition pulse and ignition sequence by standard diagnosis.
[Standard Diagnosis] Screen
If this massage appears frequently after checking above items, contact your Shimadzu sales/service representative.